Peumus boldus (leaf) - Revision history

Admin: add PlantaPhile references

2015-05-05T20:06:09Z

add PlantaPhile references

Admin: add askbox

2014-06-02T20:58:45Z

add askbox

Staffer: Voucher added

2014-03-26T06:34:35Z

Voucher added

Staffer at 01:54, 16 March 2014

2014-03-16T01:54:49Z

Staffer: Nomenclature updated

2014-03-14T19:21:06Z

Nomenclature updated

Admin: updated to new layout

2014-02-18T18:39:55Z

updated to new layout

AHPAStaff: addition of hptlc info.--jd

2013-06-25T00:12:55Z

addition of hptlc info.--jd

New page

=Introduction=
[[Category:NoIntro]]

=Macroscopic Entries=
[[Category:NoMacroscopy]]

=Microscopic Entries=
[[Category:NoMicroscopy]]

=HPTLC Entries=
{{HPTLC | source=HPTLC Association
| companyimage=HPTLC-assoc-Logo-farbig-Text-schwarz-300x47.png
| companyURL=http://www.hptlc-association.org/
| mainimage=Peumus boldus-UV 254 nm-hptclc-association.png
| caption1=Boldo (leaf) HPTLC ID - UV 254 nm
| description=Boldo (leaf) (''Peumus boldus'')
| image2=Peumus boldus-Iodine reagent, white RT-hptclc-association.png
| caption2=Boldo (leaf) HPTLC ID - Iodine reagent, white RT
|
| stationaryphase=Stationary phase, i.e. Silica gel 60, F254
| mobilephase=Diethyl amine, methanol, toluene 10:10:80 (v/v/v)
| prep=Sample: Mix 1 g of powdered sample with 10 mL of methanol and sonicate for 10 minutes, then centrifuge or filter the solutions and use the supernatants / filtrates as test solutions.

Derivatization reagent: 1% iodine reagent; Preparation: 2 g iodine in 200 mL of ethanol; Use: Dip (time 0, speed 5), heat at 100 °C for 3 minutes.
| detection=Saturated chamber; developing distance 70 mm from lower edge; relative humidity 33%
| referencesamples=Reference: Dissolve 2 mg of boldine in 5 mL of methanol. Dissolve 20 mg of hyoscine hydrobromide in 5 mL of methanol.
|
| lanes=Lanes, from left to right (Track, Volume, Sample):
# 2 µL Boldo leaf (Ph. Eur. extraction)
# 4 µL Boldo leaf (Ph. Eur. extraction)
# 6 µL Boldo leaf (Ph. Eur. extraction)
# 4 µL Boldo leaf
# '''6 µL Boldo leaf'''
# 8 µL Boldo leaf
# 2 µL Boldine
# 2 µL Hyoscine hydrobromide
# 4 µL Boldo leaf 1
# '''6 µL Boldo leaf 1'''
# 4 µL Boldo leaf 2
# '''6 µL Boldo leaf 2'''
# 4 µL Boldo leaf 3
# '''6 µL Boldo leaf 3'''
# 2 µL Boldine, hyoscine hydrobromide

| notes=''Images presented in this entry are examples and are not intended to be used as basis for setting specifications for quality control purposes.''

System suitability test (UV 254 nm): Boldine: a quenching zone at Rf ~ 0.28; Hyoscine hydrobromide: a weak quenching zone at Rf ~ 0.52

Identification: Compare result with reference images. The fingerprint of the test solution is similar to that of the corresponding botanical reference sample. Additional weak zones may be present. Under white light the chromatogram of the test solution shows a brown zone corresponding to boldine at Rf ~ 0.28. Above this zone there are three brownish zones at Rf ~ 0.33, 0.40 and 0.50, and two green zones at Rf ~ 0.61 and 0.74.

| }}

=Other Points of Interest=

[[Category:Blank2]]

← Older revision		Revision as of 20:06, 5 May 2015
Line 27:		Line 27:

	=Macroscopic Characteristics=		=Macroscopic Characteristics=
		+	{{ Media2 \| cat=Macroscopy
		+	\| source=PlantaPhile
		+	\| mainimage=PlantaPhile - 216.jpg
		+	\| companyimage=PlantaPhile logo.jpg
		+	\| companyURL=http://plantaphile.com/

		+	\| source2=PlantaPhile
		+	\| image2=PlantaPhile - 1806.jpg
		+	\| companyimage2=PlantaPhile logo.jpg
		+	\| companyURL2=http://plantaphile.com/
		+	\| }}
	=Microscopic Characteristics=		=Microscopic Characteristics=

← Older revision		Revision as of 20:58, 2 June 2014
Line 1:		Line 1:
−	{{DISPLAYTITLE:''Peumus boldus'' (leaf)}}	+	{{DISPLAYTITLE:''Peumus boldus'' (leaf)}} {{askbox\|herb=''Peumus boldus''}}
	=Nomenclature=		=Nomenclature=

← Older revision		Revision as of 06:34, 26 March 2014
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	=Botanical Voucher Specimen=		=Botanical Voucher Specimen=
		+
		+	{{Media \|cat=Voucher
		+
		+	\| source=MOBOT, Tropicos.org
		+	\| mainimage=Peumus_boldus_Tropicos_100003144_(S).jpg
		+	\| companyimage=TropicosLogo.gif
		+	\| companyURL=http://www.tropicos.org/Image/100003144
		+	\| reference=Tropicos.org. Missouri Botanical Garden. 26 Mar 2014 <http://www.tropicos.org/Image/100003144>
		+
		+	\| }}

	=Organoleptic Characteristics=		=Organoleptic Characteristics=

@@ Line 16: / Line 16: @@
 =Organoleptic Characteristics=
-=Macroscopic Descriptions=
+=Macroscopic Characteristics=
 =Microscopic Characteristics=

@@ Line 1: / Line 1: @@
 {{DISPLAYTITLE:''Peumus boldus'' (leaf)}}
 =Nomenclature=
 =Botanical Voucher Specimen=

@@ Line 1: / Line 1: @@
-=Introduction=
+{{DISPLAYTITLE:''Peumus boldus'' (leaf)}}
-[[Category:NoIntro]]
+=Nomenclature=
-=Macroscopic Entries=
+=Botanical Voucher Specimen=
-[[Category:NoMacroscopy]]
-=Microscopic Entries=
+=Organoleptic Characteristics=
-[[Category:NoMicroscopy]]
-=HPTLC Entries=
+=Macroscopic Descriptions=
 {{HPTLC | source=HPTLC Association
               | companyimage=HPTLC-assoc-Logo-farbig-Text-schwarz-300x47.png
@@ Line 51: / Line 53: @@
               | }}
-=Other Points of Interest=
+<references />
+[[Category:Botanical]]
-[[Category:Blank2]]