Rosmarinus officinalis (aerial parts) - Revision history

Admin: add PlantaPhile references

2015-04-28T18:30:36Z

add PlantaPhile references

Admin: add USD 1918 information (organoleptic and macroscopic)

2015-04-07T15:08:42Z

add USD 1918 information (organoleptic and macroscopic)

Admin: add askbox

2014-06-02T21:05:52Z

add askbox

Staffer at 00:38, 27 March 2014

2014-03-27T00:38:58Z

Staffer: Voucher added

2014-03-26T06:53:38Z

Voucher added

Staffer: Various title corrections, Source additions

2014-03-16T02:21:42Z

Various title corrections, Source additions

Staffer: Nomenclature updated

2014-03-14T21:33:50Z

Nomenclature updated

AHPAStaff: addition of hptlc info.--jd

2013-06-25T23:53:42Z

addition of hptlc info.--jd

New page

=Introduction=
[[Category:NoIntro]]

=Macroscopic Entries=
[[Category:NoMacroscopy]]

=Microscopic Entries=
[[Category:NoMicroscopy]]

=HPTLC Entries=
{{HPTLC | source=HPTLC Association
| companyimage=HPTLC-assoc-Logo-farbig-Text-schwarz-300x47.png
| companyURL=http://www.hptlc-association.org/
| mainimage=Rosmarinus officinalis oil-hptlc-association.png
| caption1=Rosemary oil (aerial parts) HPTLC ID - Anisaldehyde reagent, white RT
| description=Rosemary oil (aerial parts) (''Rosmarinus officinalis'')
|
| stationaryphase=Stationary phase, i.e. Silica gel 60, F254
| mobilephase=Ethyl acetate, toluene 5:95 (v/v)
| prep=Sample: Dissolve 20 µL of essential oil in 1 mL of toluene. Optional: mix 0.5 g of powdered dry Rosemary leaf with 5 mL of toluene and sonicate for 10 min, then centrifuge or filter the solutions and use the supernatants/filtrates as test solution.

Derivatization reagent: Anisaldehyde reagent, Preparation: 170 mL of ice-cooled methanol are mixed with 20 mL of acetic acid, 10 mL of sulfuric acid and 1 mL of anisaldehyde, Use: Dip (time 0, speed 5), heat at 100°C for 5 min.
| detection=Saturated chamber; developing distance 70 mm from lower edge; relative humidity 33%
| referencesamples=Reference: Individually dissolve 1 mg of borneol and 1 mg of bornyl acetate in 1 mL of methanol. Optional: Dissolve 10 µL of cineole in 1 mL of methanol.
|
| lanes=Lanes, from left to right (Track, Volume, Sample):
# 1 µL Rosemary oil
# '''3 µL Rosemary oil'''
# 5 µL Rosemary oil
# 2 µL Borneol
# 2 µL Bornyl acetate
# 5 µL Cineole
# 3 µL Rosemary oil CT Campher Ph.Eur. 5.0
# 3 µL Rosemary oil CT Cineole
# 1 µL Rosemary oil Ph.Eur 4.0
# 5 µL Rosemary leaf #1
# 5 µL Rosemary leaf #2
# 5 µL Rosemary leaf #3
# 5 µL Rosemary leaf #4
# 5 µL Rosemary leaf from Peru
# 5 µL Rosemary leaf from Croatia

| notes=''Images presented in this entry are examples and are not intended to be used as basis for setting specifications for quality control purposes.''

System suitability test: Borneol: brownish zone at ~ 0.21; Bornyl acetate: brown zone at ~ 0.54.

Identification: Compare result with reference images. The fingerprint of the test solution is similar to that of the corresponding botanical reference sample. Additional weak zones may be present. The chromatogram of the test solution shows a purple zone in the upper third. At the position of reference bornyl acetate there is a yellowish brown zone. Below this zone a purple zone is detected. At the position of reference cineole there is a greyish violet zone. At the position of reference borneol a yellowish brown zone is seen, just above and below this zone there is each a greyish violet zone.

| }}

=Other Points of Interest=

[[Category:Blank2]]

@@ Line 37: / Line 37: @@
 {{Macroscopy | source=United States Dispensatory (1918)
 | description=Rosemary is a small evergreen shrub, with an erect stem, divided into many long, slender, ash-colored branches. The leaves are numerous, sessile, opposite, about 2.5 cm. long, rigid, linear, entire, obtuse at the summit, folded backward at the edges, of a firm consistence, smooth and green on the upper surface, whitish, woolly, and glandular beneath. The flowers are axillary, pale blue or white.}}
 |}

@@ Line 25: / Line 25: @@
 =Organoleptic Characteristics=
 =Macroscopic Characteristics=
 =Microscopic Characteristics=

← Older revision		Revision as of 21:05, 2 June 2014
Line 1:		Line 1:
−	{{DISPLAYTITLE:''Rosmarinus officinalis'' (aerial parts) }}	+	{{DISPLAYTITLE:''Rosmarinus officinalis'' (aerial parts) }} {{askbox\|herb=''Rosmarinus officinalis''}}
	=Nomenclature=		=Nomenclature=

@@ Line 19: / Line 19: @@
               | mainimage=Rosmarinus_officinalis_Tropicos_100002347_(S).jpg
               | companyimage=TropicosLogo.gif
-              | companyURL=http://www.tropicos.org/image/100002347
+              | companyURL=http://www.tropicos.org/Image/100002347
-              | reference=Tropicos.org. Missouri Botanical Garden. 26 Mar 2014 <http://www.tropicos.org/image/100002347>
+              | reference=Tropicos.org. Missouri Botanical Garden. 26 Mar 2014 <http://www.tropicos.org/Image/100002347>
               | }}

← Older revision		Revision as of 06:53, 26 March 2014
Line 13:		Line 13:

	=Botanical Voucher Specimen=		=Botanical Voucher Specimen=
		+
		+	{{Media \|cat=Voucher
		+
		+	\| source=MOBOT, Tropicos.org
		+	\| mainimage=Rosmarinus_officinalis_Tropicos_100002347_(S).jpg
		+	\| companyimage=TropicosLogo.gif
		+	\| companyURL=http://www.tropicos.org/image/100002347
		+	\| reference=Tropicos.org. Missouri Botanical Garden. 26 Mar 2014 <http://www.tropicos.org/image/100002347>
		+
		+	\| }}
		+
	=Organoleptic Characteristics=		=Organoleptic Characteristics=

@@ Line 1: / Line 1: @@
 =Nomenclature=
@@ Line 11: / Line 12: @@
 |notes= }}
-=Macroscopic Entries=
+=Botanical Voucher Specimen=
-[[Category:NoMacroscopy]]
+=Organoleptic Characteristics=
-=Microscopic Entries=
+=Macroscopic Characteristics=
-[[Category:NoMicroscopy]]
+=Microscopic Characteristics=
 {{HPTLC | source=HPTLC Association
               | companyimage=HPTLC-assoc-Logo-farbig-Text-schwarz-300x47.png
@@ Line 58: / Line 60: @@
               | }}
-=Other Points of Interest=
+=Supplementary Information=
+=Sources=
-[[Category:Blank2]]
+<references />