Angelica dahurica (root)

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=HPTLC Entries=
 
=HPTLC Entries=
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{{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories
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            | description=Fragrant Angelica (root) (''Angelica dahurica'')
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            | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg
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            | companyURL=http://www.alkemist.com
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            | mainimage=Angelica_dahurica_-_Alkemists_Laboratories.jpg
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            | caption1=''Angelica dahurica'' HPTLC ID - 5% Methanolic Sulfuric Acid Reagent UV 365 nm
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            | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates
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            | mobilephase=toluene: ethyl acetate: HCOOH [9/1/0.1]
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            | prep=0.3 g + 3 ml CH3OH sonicated + heated @ 50° C ~ 1 hr
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            | detection=5% Methanolic H2SO4 -> UV 365 nm
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            | lanes= Lanes, from left to right (Track, Volume, Sample):
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# 2 μL Imperatorin ~0.1% Methanol
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# 3 μL ''Angelica dahurica''-1 (root)
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# 3 μL ''Angelica dahurica''-2 (root)
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# 3 μL ''Angelica dahurica''-3 (root)
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# 3 μL ''Angelica dahurica''-4 (root)
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# 3 μL ''Angelica sinensis''-1 (root)
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# 3 μL ''Angelica archangelica''-1 (root)
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# 2 μL Ligustilide ~0.1% Methanol
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 +
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA.
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            | reference=Adapted from Japanese Official Monographs part III
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            | }}
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=Other Points of Interest=
 
=Other Points of Interest=
 
[[Category:blank]]
 
[[Category:blank]]

Revision as of 00:22, 30 November 2012

Contents

Introduction

Macroscopic Entries

Microscopic Entries

Parenchyma packed with starch granule of various sizes observed at 400x with Acidified Chloral Hydrate Glycerol Solution.

Source: Elan M. Sudberg, Alkemist Laboratories [1]

AP-LOGO-Laboratories Crop - Copy.jpg
Angelica dahurica-1 - Alkemist Laboratories.jpg



HPTLC Entries

AP-LOGO-Laboratories Crop - Copy.jpg
(thumbnail)
Angelica dahurica HPTLC ID - 5% Methanolic Sulfuric Acid Reagent UV 365 nm

Fragrant Angelica (root) (Angelica dahurica)

Lane Assignments Lanes, from left to right (Track, Volume, Sample):

  1. 2 μL Imperatorin ~0.1% Methanol
  2. 3 μL Angelica dahurica-1 (root)
  3. 3 μL Angelica dahurica-2 (root)
  4. 3 μL Angelica dahurica-3 (root)
  5. 3 μL Angelica dahurica-4 (root)
  6. 3 μL Angelica sinensis-1 (root)
  7. 3 μL Angelica archangelica-1 (root)
  8. 2 μL Ligustilide ~0.1% Methanol

Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. 

Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates 

Mobile Phase toluene: ethyl acetate: HCOOH [9/1/0.1] 

Sample Preparation Method 0.3 g + 3 ml CH3OH sonicated + heated @ 50° C ~ 1 hr 

Detection Method 5% Methanolic H2SO4 -> UV 365 nm 

Reference see Adapted from Japanese Official Monographs part III


Source: Elan M. Sudberg, Alkemist Laboratories [2]

Other Points of Interest


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