Foeniculum vulgare (seed)
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=HPTLC Entries= | =HPTLC Entries= | ||
+ | {{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories | ||
+ | | description=Fennel (seed) (''Foeniculum vulgare'') | ||
+ | | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg | ||
+ | | companyURL=http://www.alkemist.com | ||
+ | | mainimage=Foeniculum vulgare - Alkemists Laboratories.jpg | ||
+ | | caption1=''Foeniculum vulgare'' HPTLC ID - Vanillin/H2SO4 Reagent UV 365 nm | ||
+ | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
+ | | mobilephase=toluene: ethyl acetate [9.5/0.5] | ||
+ | | prep=0.5g+5ml dichloromethane, sonicate/centrifuge/decant, evaporate to dryness with N2, qs 1.0 ml Toluene | ||
+ | | detection=Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm | ||
+ | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
+ | # 1 μL Eugenol ~0.1% in CH3OH | ||
+ | # 3 μL ''Foeniculum vulgare''-1 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-2 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-3 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-3 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-4 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-5 (seed) | ||
+ | # 3 μL ''Foeniculum vulgare''-6 (seed) | ||
+ | |||
+ | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Pharmaceuticals, Costa Mesa, CA. | ||
+ | |||
+ | | reference=British Pharmacopoeia, 2003 | ||
+ | | }} | ||
=Other Points of Interest= | =Other Points of Interest= | ||
[[Category:blank]] | [[Category:blank]] |
Revision as of 20:48, 22 October 2012
Contents |
Introduction
Macroscopic Entries
Microscopic Entries
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HPTLC Entries
Fennel (seed) (Foeniculum vulgare) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Pharmaceuticals, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase toluene: ethyl acetate [9.5/0.5] Sample Preparation Method 0.5g+5ml dichloromethane, sonicate/centrifuge/decant, evaporate to dryness with N2, qs 1.0 ml Toluene Detection Method Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm Reference see British Pharmacopoeia, 2003
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Other Points of Interest
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