Glycine max (bean)
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=HPTLC Entries= | =HPTLC Entries= | ||
+ | {{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories | ||
+ | | description=Soy (bean) (''Glycine max'') | ||
+ | | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg | ||
+ | | companyURL=http://www.alkemist.com | ||
+ | | mainimage=Glycine_max_-_Alkemists_Laboratories.jpg | ||
+ | | caption1=''Glycine max'' HPTLC ID - Vanillin Sulfuric Acid Reagent UV 365 nm | ||
+ | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
+ | | mobilephase=ethyl acetate: Acetic acid: CH3OH: H2O [6/1.5/1.5/1] | ||
+ | | prep=0.3 g + 3 ml 70% grain EtOH sonicate/heat @ 50° C ~ 1/2 hr | ||
+ | | detection=Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm | ||
+ | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
+ | # 3 μL Aescin ~0.1% in Methanol | ||
+ | # 3 μL ''Glycine max''-1 | ||
+ | # 3 μL ''Glycine max''-2 | ||
+ | # 3 μL ''Glycine max''-3 | ||
+ | # 3 μL ''Glycine max''-3 | ||
+ | # 3 μL ''Glycine max''-4 | ||
+ | # 3 μL ''Glycine max''-5 | ||
+ | # 3 μL Daidzein ~0.1% in Methanol | ||
+ | |||
+ | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | ||
+ | |||
+ | | reference=Method Developed by Alkemists Laboratories | ||
+ | | }} | ||
+ | |||
=Other Points of Interest= | =Other Points of Interest= | ||
[[Category:blank]] | [[Category:blank]] |
Revision as of 00:09, 30 November 2012
Contents |
Introduction
Macroscopic Entries
Microscopic Entries
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HPTLC Entries
Soy (bean) (Glycine max) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase ethyl acetate: Acetic acid: CH3OH: H2O [6/1.5/1.5/1] Sample Preparation Method 0.3 g + 3 ml 70% grain EtOH sonicate/heat @ 50° C ~ 1/2 hr Detection Method Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm Reference see Method Developed by Alkemists Laboratories
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Other Points of Interest
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