Lycium barbarum (fruit)

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=HPTLC Entries=
 
=HPTLC Entries=
 +
{{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories
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            | description=Goji (fruit) (''Lycium barbarum'')
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            | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg
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            | companyURL=http://www.alkemist.com
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            | mainimage=Lycium_barbarum_-_Alkemists_Laboratories.jpg
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            | caption1=''Lycium barbarum'' HPTLC ID - Vanillin Sulfuric Acid Reagent - UV 365 nm
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            | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates
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            | mobilephase=ethyl acetate: CHCl3: HCOOH [6/4/2]
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            | prep=0.3 g + 3 ml 80% CH3OH sonicated + heated @ 50° C ~ 1 hr
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            | detection=Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm
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            | lanes= Lanes, from left to right (Track, Volume, Sample):
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# 2 μL Catechin ~0.1% in Methanol
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# 3 μL ''Lycium chinense''-1 (fruit)
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# 3 μL ''Lycium barbarum''-1 (fruit)
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# 3 μL ''Lycium barbarum''-2 (fruit)
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# 3 μL ''Lycium barbarum''-2 (fruit)
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# 3 μL ''Lycium barbarum''-3 (fruit)
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# 3 μL ''Lycium barbarum''-4 (fruit)
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# 2 μL Gallic Acid ~0.1% in Methanol
 +
 +
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA.
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            | reference=Pharmacopoeia of The Peoples Republic of China, Volume 1, 2005
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            | }}
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=Other Points of Interest=
 
=Other Points of Interest=
 
[[Category:blank]]
 
[[Category:blank]]

Revision as of 00:36, 30 November 2012

Contents

Introduction

Macroscopic Entries

Microscopic Entries

Lignified cells of the testa observed at 400x with Acidified Chloral Hydrate Glycerol Solution.

Source: Elan M. Sudberg, Alkemist Laboratories [1]

AP-LOGO-Laboratories Crop - Copy.jpg
Lycium barbarum - Alkemist Laboratories.jpg


HPTLC Entries

AP-LOGO-Laboratories Crop - Copy.jpg
(thumbnail)
Lycium barbarum HPTLC ID - Vanillin Sulfuric Acid Reagent - UV 365 nm

Goji (fruit) (Lycium barbarum)

Lane Assignments Lanes, from left to right (Track, Volume, Sample):

  1. 2 μL Catechin ~0.1% in Methanol
  2. 3 μL Lycium chinense-1 (fruit)
  3. 3 μL Lycium barbarum-1 (fruit)
  4. 3 μL Lycium barbarum-2 (fruit)
  5. 3 μL Lycium barbarum-2 (fruit)
  6. 3 μL Lycium barbarum-3 (fruit)
  7. 3 μL Lycium barbarum-4 (fruit)
  8. 2 μL Gallic Acid ~0.1% in Methanol

Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. 

Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates 

Mobile Phase ethyl acetate: CHCl3: HCOOH [6/4/2] 

Sample Preparation Method 0.3 g + 3 ml 80% CH3OH sonicated + heated @ 50° C ~ 1 hr 

Detection Method Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm 

Reference see Pharmacopoeia of The Peoples Republic of China, Volume 1, 2005


Source: Elan M. Sudberg, Alkemist Laboratories [2]

Other Points of Interest


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