Magnolia officinalis (bark)

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=HPTLC Entries=
 
=HPTLC Entries=
 +
{{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories
 +
            | description=Magnolia (bark) (''Magnolia officinalis'')
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            | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg
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            | companyURL=http://www.alkemist.com
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            | mainimage=Magnolia_officinalis_-_Alkemists_Laboratories.jpg
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            | caption1=''Magnolia officinalis'' HPTLC ID - 10% Ethanolic H2SO4 visible light
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            | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates
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            | mobilephase=cyclohexane: ethyl acetate: HCOOH [6/4/0.2]
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            | prep=0.3g+3mL 70% grain EtOH sonicate/heat @~50° C ~ 1/2 hr
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            | detection=10% Ethanolic H2SO4 -> 115° C 15 min -> visible light
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            | lanes= Lanes, from left to right (Track, Volume, Sample):
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# 3 μL Magnolol ~ 0.1% in Methanol
 +
# 3 μL ''Magnolia officinalis''-1
 +
# 3 μL ''Magnolia officinalis''-2
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# 3 μL ''Magnolia officinalis''-3
 +
# 3 μL ''Magnolia officinalis''-3
 +
# 4 μL ''Magnolia officinalis''-4
 +
# 2 μL ''Magnolia officinalis''-4
 +
# 3 μL Honokiol ~ 0.1% in Methanol
 +
 +
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA.
 +
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            | reference=Pharmacopoeia of The Peoples Republic of China, Volume 1, 1997
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            | }}
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=Other Points of Interest=
 
=Other Points of Interest=
 
[[Category:blank]]
 
[[Category:blank]]

Revision as of 23:11, 4 December 2012

Contents

Introduction

Macroscopic Entries

Microscopic Entries

Cells containing yellow-brown oil observed at 400x with Acidified Chloral Hydrate Glycerol Solution.

Source: Elan M. Sudberg, Alkemist Laboratories [1]

AP-LOGO-Laboratories Crop - Copy.jpg
Magnolia officinalis - Alkemist Laboratories.jpg


HPTLC Entries

AP-LOGO-Laboratories Crop - Copy.jpg
(thumbnail)
Magnolia officinalis HPTLC ID - 10% Ethanolic H2SO4 visible light

Magnolia (bark) (Magnolia officinalis)

Lane Assignments Lanes, from left to right (Track, Volume, Sample):

  1. 3 μL Magnolol ~ 0.1% in Methanol
  2. 3 μL Magnolia officinalis-1
  3. 3 μL Magnolia officinalis-2
  4. 3 μL Magnolia officinalis-3
  5. 3 μL Magnolia officinalis-3
  6. 4 μL Magnolia officinalis-4
  7. 2 μL Magnolia officinalis-4
  8. 3 μL Honokiol ~ 0.1% in Methanol

Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. 

Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates 

Mobile Phase cyclohexane: ethyl acetate: HCOOH [6/4/0.2] 

Sample Preparation Method 0.3g+3mL 70% grain EtOH sonicate/heat @~50° C ~ 1/2 hr 

Detection Method 10% Ethanolic H2SO4 -> 115° C 15 min -> visible light 

Reference see Pharmacopoeia of The Peoples Republic of China, Volume 1, 1997


Source: Elan M. Sudberg, Alkemist Laboratories [2]

Other Points of Interest


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