Phyllanthus emblica (fruit)
m (added volume of reference sample applied in each lane and image caption) |
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| companyURL=http://www.alkemist.com | | companyURL=http://www.alkemist.com | ||
| mainimage=Phyllanthus_emblica_-_Alkemists_Laboratories2.jpg | | mainimage=Phyllanthus_emblica_-_Alkemists_Laboratories2.jpg | ||
| − | | caption1=''Phyllanthus emblica'' | + | | caption1=''Phyllanthus emblica'' HPTLC ID - 10% Methanolic Sulfuric Acid UV 365 nm |
| stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
| mobilephase=toluene: ethyl formate: formic acid [5/4/1] | | mobilephase=toluene: ethyl formate: formic acid [5/4/1] | ||
| Line 25: | Line 25: | ||
| detection=10% Methanolic H2SO4 -> 115° C 15 min -> UV 365 nm | | detection=10% Methanolic H2SO4 -> 115° C 15 min -> UV 365 nm | ||
| lanes= Lanes, from left to right (Track, Volume, Sample): | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
| − | # | + | # 2 μL Gallic Acid ~0.1% in CH3OH |
| − | # | + | # 2 μL ''Phyllanthus emblica''-1 |
| − | # | + | # 2 μL ''Phyllanthus emblica''-2 |
| − | # | + | # 1 μL ''Phyllanthus emblica''-3 |
| − | # | + | # 1 μL ''Phyllanthus emblica''-3 |
| − | # | + | # 3 μL ''Phyllanthus emblica''-4 |
| − | # | + | # 3 μL ''Phyllanthus emblica''-4 |
| − | # | + | # 2 μL Gallic Acid ~0.1% in CH3OH |
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | ||
Revision as of 22:28, 23 October 2012
Contents |
Introduction
Macroscopic Entries
Microscopic Entries
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HPTLC Entries
 
Amla (fruit) (Phyllanthus emblica) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase toluene: ethyl formate: formic acid [5/4/1] Sample Preparation Method 0.3g+3mL 70% grain EtOH sonicate/heat @ 50° C ~ 1/2 hr Detection Method 10% Methanolic H2SO4 -> 115° C 15 min -> UV 365 nm Reference see Indian Herbal Pharmacopoeia Vol 2 1999
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Other Points of Interest
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