Piper methysticum (rhizome)
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=Microscopic Entries= | =Microscopic Entries= | ||
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+ | {{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories | ||
+ | | description=Kava (rhizome) (''Piper methysticum'') | ||
+ | | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg | ||
+ | | companyURL=http://www.alkemist.com | ||
+ | | mainimage=Piper_methysticum_-_Alkemists_Laboratories.jpg | ||
+ | | caption1=''Piper methysticum'' HPTLC ID - Vanillin Sulfuric Acid UV 365 nm | ||
+ | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
+ | | mobilephase=H2O: acetonitrile: CH3OH: AcCOOH: >Reverse Phase!!!! [4/3/3/0.01/] | ||
+ | | prep=0.3g+3mL 70% grain EtOH sonicate/heat @ 50° C ~ 1/2 hr | ||
+ | | detection=Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm | ||
+ | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
+ | # 3 μL Kavain | ||
+ | # 3 μL ''Piper methysticum''-1 (rhizome) | ||
+ | # 3 μL ''Piper methysticum''-2 (rhizome) | ||
+ | # 3 μL ''Piper methysticum''-3 (rhizome) | ||
+ | # 3 μL ''Piper methysticum''-3 (rhizome) | ||
+ | # 3 μL ''Piper methysticum''-4 (rhizome) | ||
+ | # 3 μL ''Piper methysticum''-5 (rhizome) | ||
+ | # 3 μL Kavain | ||
+ | |||
+ | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | ||
+ | |||
+ | | reference=Plant Drug Analysis, Wagner, H., 1996 | ||
+ | | }} | ||
+ | |||
=Other Points of Interest= | =Other Points of Interest= | ||
[[Category:blank]] | [[Category:blank]] |
Revision as of 18:55, 23 October 2012
Contents |
Introduction
Macroscopic Entries
Microscopic Entries
HPTLC Entries
Kava (rhizome) (Piper methysticum) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase H2O: acetonitrile: CH3OH: AcCOOH: >Reverse Phase!!!! [4/3/3/0.01/] Sample Preparation Method 0.3g+3mL 70% grain EtOH sonicate/heat @ 50° C ~ 1/2 hr Detection Method Vanillin/H2SO4 Reagent -> 110° C 5 min -> UV 365 nm Reference see Plant Drug Analysis, Wagner, H., 1996
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Other Points of Interest
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