Citrus paradisi (seed)
(→updates to ABC-AHP-NCNPR Botanical Adulterants Prevention Program program title) |
|||
| (7 intermediate revisions by 3 users not shown) | |||
| Line 1: | Line 1: | ||
| − | = | + | {{DISPLAYTITLE:''Citrus paradisi'' (seed) }} {{askbox|herb=''Citrus paradisi''}} |
| − | =Macroscopic | + | =Nomenclature= |
| − | =Microscopic | + | {{nomenclature | binomial=Citrus x paradisi |
| − | =HPTLC | + | |authority=Macfad. |
| − | = | + | |family=Rutaceae |
| − | + | |scn=grapefruit | |
| − | [ | + | |syn= |
| + | |ayurvedic= | ||
| + | |pinyin= | ||
| + | |aka= | ||
| + | |notes= }} | ||
| + | |||
| + | =Botanical Voucher Specimen= | ||
| + | {{Media |cat=Voucher | ||
| + | |companyimage=Starr herbarium logo.png | ||
| + | | companyURL=http://sciweb.nybg.org/science2/VirtualHerbarium.asp | ||
| + | |mainimage=Citrus paradisi Macfad. - Starr - v-162-01341949.jpg | ||
| + | |caption1=''Citrus paradisi'' Macfad. | ||
| + | |source=Images courtesy of the C.V. Starr Virtual Herbarium of the New York Botanical Garden | ||
| + | |}} | ||
| + | =Organoleptic Characteristics= | ||
| + | |||
| + | =Macroscopic Characteristics= | ||
| + | =Microscopic Characteristics= | ||
| + | =High Performance Thin Layer Chromatographic Identification= | ||
| + | |||
| + | {{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories | ||
| + | | description=Grapefruit (seed) (''Citrus paradisi'') | ||
| + | | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg | ||
| + | | companyURL=http://www.alkemist.com | ||
| + | | mainimage=Citrus paradisi seed - Alkemists Laboratories.jpg | ||
| + | | caption1=''Citrus paradisi'' HPTLC ID - 10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm | ||
| + | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
| + | | mobilephase=CHCl3: CH3OH: HCOOH: H2O [6/2/1.4/0.1] | ||
| + | | prep=0.3 g + 3 ml CH3OH sonicate/heat @ 50° C ~ 1/2 hr | ||
| + | | detection=10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm | ||
| + | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
| + | # 3 μL Hesperidin, Hesperitin ~0.1% in CH3OH | ||
| + | # 3 μL ''Citrus paradisi''-1 (seed) | ||
| + | # 3 μL ''Citrus paradisi''-2 (seed) | ||
| + | # 3 μL ''Citrus paradisi''-3 (seed) | ||
| + | # 3 μL ''Citrus paradisi''-3 (seed) | ||
| + | # 3 μL ''Citrus paradisi''-4 (seed) | ||
| + | # 3 μL ''Citrus paradisi''-5 (seed) | ||
| + | # 3 μL Naringin, Naringenin ~0.1% in CH3OH | ||
| + | |||
| + | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | ||
| + | |||
| + | | reference=Method Developed by Alkemists Laboratories | ||
| + | | }} | ||
| + | |||
| + | =Supplementary Information= | ||
| + | |||
| + | == ABC-AHP-NCNPR Botanical Adulterants Prevention Program Laboratory Guidance == | ||
| + | {{Botanical | source=ABC-AHP-NCNPR Botanical Adulterants Prevention Program | ||
| + | | companyimage=BAPP-logo-2018-2line-LOW2.jpg | ||
| + | | companyURL=http://cms.herbalgram.org/BAP/LGD/GrapefruitSeedExtractLabGuidanceDocument.html | ||
| + | | description=Grapefruit (seed extract) (''Citrus paradisi'') | ||
| + | | characteristics=This ABC-AHP-NCNPR Botanical Adulterants Prevention Program [http://cms.herbalgram.org/BAP/LGD/GrapefruitSeedExtractLabGuidanceDocument.html Laboratory Guidance Document] presents an overview and comparison of various analytical technologies and methods used to differentiate between authentic grapefruit seed extract ingredients and non-authentic materials, with particular discussion of synthetic microbicidal compounds identified in non-authentic materials, authentic grapefruit seed extract components, and a detailed literature review of methods (including sample characterization via TLC, HPLC-UV, HPLC-MS, GC-MS, and others). | ||
| + | }} | ||
| + | |||
| + | =Sources= | ||
| + | |||
| + | <references /> | ||
Latest revision as of 17:38, 17 October 2018
Contents |
Nomenclature
Citrus x paradisi Macfad. Rutaceae
Standardized common name (English): grapefruit
Botanical Voucher Specimen
|
|
Organoleptic Characteristics
Macroscopic Characteristics
Microscopic Characteristics
High Performance Thin Layer Chromatographic Identification
|
Grapefruit (seed) (Citrus paradisi) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase CHCl3: CH3OH: HCOOH: H2O [6/2/1.4/0.1] Sample Preparation Method 0.3 g + 3 ml CH3OH sonicate/heat @ 50° C ~ 1/2 hr Detection Method 10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm Reference see Method Developed by Alkemists Laboratories
|
Supplementary Information
ABC-AHP-NCNPR Botanical Adulterants Prevention Program Laboratory Guidance
Grapefruit (seed extract) (Citrus paradisi)
General Characteristics This ABC-AHP-NCNPR Botanical Adulterants Prevention Program Laboratory Guidance Document presents an overview and comparison of various analytical technologies and methods used to differentiate between authentic grapefruit seed extract ingredients and non-authentic materials, with particular discussion of synthetic microbicidal compounds identified in non-authentic materials, authentic grapefruit seed extract components, and a detailed literature review of methods (including sample characterization via TLC, HPLC-UV, HPLC-MS, GC-MS, and others).
Source: ABC-AHP-NCNPR Botanical Adulterants Prevention Program [3]
Sources
- ↑ Images courtesy of the C.V. Starr Virtual Herbarium of the New York Botanical Garden http://sciweb.nybg.org/science2/VirtualHerbarium.asp
- ↑ Elan M. Sudberg, Alkemist Laboratories http://www.alkemist.com
- ↑ ABC-AHP-NCNPR Botanical Adulterants Prevention Program http://cms.herbalgram.org/BAP/LGD/GrapefruitSeedExtractLabGuidanceDocument.html