Citrus paradisi (seed)
From AHPA Botanical Identity References Compendium
(Difference between revisions)
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=Microscopic Entries= | =Microscopic Entries= | ||
=HPTLC Entries= | =HPTLC Entries= | ||
+ | {{HPTLC | source=Elan M. Sudberg, Alkemist Laboratories | ||
+ | | description=Grapefruit (seed) (''Citrus paradisi'') | ||
+ | | companyimage=AP-LOGO-Laboratories Crop - Copy.jpg | ||
+ | | companyURL=http://www.alkemist.com | ||
+ | | mainimage=Citrus paradisi seed - Alkemists Laboratories.jpg | ||
+ | | caption1=''Citrus paradisi'' HPTLC ID - 10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm | ||
+ | | stationaryphase=Silica gel 60, F254, 10 x 10 cm HPTLC plates | ||
+ | | mobilephase=CHCl3: CH3OH: HCOOH: H2O [6/2/1.4/0.1] | ||
+ | | prep=0.3 g + 3 ml CH3OH sonicate/heat @ 50° C ~ 1/2 hr | ||
+ | | detection=10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm | ||
+ | | lanes= Lanes, from left to right (Track, Volume, Sample): | ||
+ | # 3 μL Hesperidin, Hesperitin ~0.1% in CH3OH | ||
+ | # 3 μL ''Citrus paradisi''-1 (seed) | ||
+ | # 3 μL ''Citrus paradisi''-2 (seed) | ||
+ | # 3 μL ''Citrus paradisi''-3 (seed) | ||
+ | # 3 μL ''Citrus paradisi''-3 (seed) | ||
+ | # 3 μL ''Citrus paradisi''-4 (seed) | ||
+ | # 3 μL ''Citrus paradisi''-5 (seed) | ||
+ | # 3 μL Naringin, Naringenin ~0.1% in CH3OH | ||
+ | |||
+ | Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. | ||
+ | |||
+ | | reference=Method Developed by Alkemists Laboratories | ||
+ | | }} | ||
+ | |||
=Other Points of Interest= | =Other Points of Interest= | ||
− | |||
[[Category:NoIntro]] | [[Category:NoIntro]] |
Revision as of 22:00, 15 March 2013
Contents |
Introduction
Macroscopic Entries
Microscopic Entries
HPTLC Entries
Grapefruit (seed) (Citrus paradisi) Lane Assignments Lanes, from left to right (Track, Volume, Sample):
Reference materials used here have been authenticated by macroscopic, microscopic &/or TLC studies according to the reference source cited below held at Alkemists Laboratories, Costa Mesa, CA. Stationary Phase Silica gel 60, F254, 10 x 10 cm HPTLC plates Mobile Phase CHCl3: CH3OH: HCOOH: H2O [6/2/1.4/0.1] Sample Preparation Method 0.3 g + 3 ml CH3OH sonicate/heat @ 50° C ~ 1/2 hr Detection Method 10% Ethanolic H2SO4-> 115° C 15 min -> UV 365 nm Reference see Method Developed by Alkemists Laboratories
|
Other Points of Interest
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